Acid Slap

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  • Application When used with aliphatic or aromatic aldehydes, this silicon amine protocol reagent enables the photomediated synthesis of thiomorpholines and rilrisucacuddtunepdiahourgtikickfid.coinfo photocatalytic cross-coupling with this SLAP Reagent, Ir[(ppy) 2 dtbbpy]PF 6 (() is used with a recommended starting combination of Lewis acids Bi(OTf) 3 and Cu(OTf) 2 prior to subsequent substrate-specific optimization.
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  • • Lewis Acid Induced Toggle from Ir(II) to Ir(IV) Pathways in Photocatalytic Reactions: Synthesis of Thiomorpholines and Thiazepanes from Aldehydes and SLAP Reagents. • Continuous Flow Synthesis of Morpholines and Oxazepanes with Silicon Amine Protocol (SLAP) Reagents and Lewis Acid Facilitated Photoredox Catalysis.
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  • Inclusion of a Lewis acid in the reaction also enables the transformation of SLAP reagents to thiomorpholines and thiazepanes. 3 Morpholines and thiomorpholines can also be accessed using the alternative organic photocatalyst 2,4,6-triphenylpyrylium tetrafluoroborate (TPP·BF4, ). 3 These conditions, particularly the use of the organic photocatalyst (TPP) and a Lewis acid additive, are.

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